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Hazard and Risk Assessment:
Procedure:
MNR35-2 (0.5 g, 0.19 mmol) in toluene (2 mL) was treated with methanesulfonic acid (0.05 mL, 0.37 mmol) and the reaction was heated to reflux for 3 hours by which time TLC had shown complete consumption of SM.
Crude - 0.045 g as a dark brown oil