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18th February 2014 @ 07:45
626 mg of KAB119.2. Dissovled in 6 mL IPA/6 mL water. Added ~6 mL water to make a slurry. Dissolved with ~6.5 mL IPA. Standing at rt. The mixture formed a semi-solid. Non-crystalline. Suspect amine wasn't pure. Attempted purification using column chromatography.