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68706870Resolution of MNR26-7 with (-)-dibenzoyl-L-tartaric acid to obtain MNR27-27 to MNR27-29
Experiments
plus.google.com-113014781212630252105Murray Robertson [b]Hazard and Risk Assessment:[/b] As for [url=http://www.ourexperiment.org/racres_pzq/2228/Resolution_of_praziquanamine_with_dipanisoylLtartaric_acid_to_obtain_SPZQamine_MNR21.html]MNR2-1[/url] MNR26-7 (0.030 g, 0.11 mmol) and [url=http://www.ourexperiment.org/racres_pzq/2289/Synthesis_of_DibenzoylLtartaric_acid_MNR61.html](-)-dibenzoyl-L-tartaric acid. 2IPA[/url] (0.05 g, 0.11 mmol) was dissolved in a isopropanol (2.5 mL). MNR27-27 - nothing else added MNR27-28 - water (0.5 mL) sdded MNR27-29 - water (0.25 mL) added The reagents went into solution with minimal heating and we left to stand, sealed, at room temperature overnight. ]]>Mnr: 21-30
Resolution of MNR26-7 with (-)-dibenzoyl-L-tartaric acid (MNR6-1) to obtain MNR27-26

Starting material from
Hydrolysis of MNR11-18 to give MNR26-7
Synthesis of (-)-Dibenzoyl-L-tartaric acid (MNR6-1)





Hazard and Risk Assessment:
As for MNR2-1

MNR26-7 (0.030 g, 0.11 mmol) and (-)-dibenzoyl-L-tartaric acid. 2IPA (0.05 g, 0.11 mmol) was dissolved in a isopropanol (2.5 mL).

MNR27-27 - nothing else added
MNR27-28 - water (0.5 mL) sdded
MNR27-29 - water (0.25 mL) added

The reagents went into solution with minimal heating and we left to stand, sealed, at room temperature overnight.
]]>2013-05-08T07:39:34+01:002013-05-08T07:39:34+01:0093055175c4a52339fa93a39569bbb5fe521-30http://www.ourexperiment.org/uri/2c2https://www.ourexperiment.org/racres_pzq/6870/Resolution_of_MNR267_with_dibenzoylLtartaric_acid_to_obtain_MNR2727_to_MNR2729.htmlhttps://www.ourexperiment.org/racres_pzq/6870/Resolution_of_MNR267_with_dibenzoylLtartaric_acid_to_obtain_MNR2727_to_MNR2729.htmlhttps://www.ourexperiment.org/racres_pzq/6870/Resolution_of_MNR267_with_dibenzoylLtartaric_acid_to_obtain_MNR2727_to_MNR2729.xmlhttps://www.ourexperiment.org/racres_pzq/6870/Resolution_of_MNR267_with_dibenzoylLtartaric_acid_to_obtain_MNR2727_to_MNR2729.pnghttps://www.ourexperiment.org/racres_pzq/6870/Resolution_of_MNR267_with_dibenzoylLtartaric_acid_to_obtain_MNR2727_to_MNR2729.xml?revision=6870https://www.ourexperiment.org/racres_pzq/6870/Resolution_of_MNR267_with_dibenzoylLtartaric_acid_to_obtain_MNR2727_to_MNR2729.xml?revision=7057
68707057Resolution of MNR26-7 with (-)-dibenzoyl-L-tartaric acid to obtain MNR27-27 to MNR27-29
Experiments
plus.google.com-113014781212630252105Murray Robertson [b]Hazard and Risk Assessment:[/b] As for [url=http://www.ourexperiment.org/racres_pzq/2228/Resolution_of_praziquanamine_with_dipanisoylLtartaric_acid_to_obtain_SPZQamine_MNR21.html]MNR2-1[/url] MNR26-7 (0.030 g, 0.11 mmol) and [url=http://www.ourexperiment.org/racres_pzq/2289/Synthesis_of_DibenzoylLtartaric_acid_MNR61.html](-)-dibenzoyl-L-tartaric acid. 2IPA[/url] (0.05 g, 0.11 mmol) was dissolved in a isopropanol (2.5 mL). MNR27-27 - nothing else added MNR27-28 - water (0.5 mL) sdded MNR27-29 - water (0.25 mL) added The reagents went into solution with minimal heating and we left to stand, sealed, at room temperature overnight.]]>Mnr: 21-30
Resolution of MNR26-7 with (-)-dibenzoyl-L-tartaric acid (MNR6-1) to obtain MNR27-26

Starting material from
Hydrolysis of MNR11-18 to give MNR26-7
Synthesis of (-)-Dibenzoyl-L-tartaric acid (MNR6-1)





Hazard and Risk Assessment:
As for MNR2-1

MNR26-7 (0.030 g, 0.11 mmol) and (-)-dibenzoyl-L-tartaric acid. 2IPA (0.05 g, 0.11 mmol) was dissolved in a isopropanol (2.5 mL).

MNR27-27 - nothing else added
MNR27-28 - water (0.5 mL) sdded
MNR27-29 - water (0.25 mL) added

The reagents went into solution with minimal heating and we left to stand, sealed, at room temperature overnight.
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