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Mnr
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Mnr: 21-30
Screening conditions for optimum resolution of MNR26-1 with (-)-dibenzoyl-L-tartaric acid (MNR6-1) to obtain R-di-methoxy-PZQamine (MNR27-x)
* As a result of mnr27-1 not working.
Hazard and Risk Assessment:
As for MNR2-1
MNR27-2
MNR26-1 (0.08 g, 0.3 mmol) and (-)-dibenzoyl-L-tartaric acid. 2IPA (0.15 g, 0.3 mmol) was dissolved in isopropanol (4 mL) in a vial and heated with the heat gun to dissolve the reagents.
Everything went into solution and the vial was left to stand at room temperature overnight.
MNR27-3
MNR26-1 (0.08 g, 0.3 mmol) and (-)-dibenzoyl-L-tartaric acid. 2IPA (0.15 g, 0.3 mmol) was dissolved in hexane (4 mL) in a vial and heated with the heat gun to dissolve the reagents.
very little went into solution and the vial was left to stand at room temperature overnight.
MNR27-4
MNR26-1 (0.08 g, 0.3 mmol) and (-)-dibenzoyl-L-tartaric acid. 2IPA (0.15 g, 0.3 mmol) was dissolved in IPA (1 mL) ans hexane(3 mL) in a vial and heated with the heat gun to dissolve the reagents.
very little went into solution and the vial was left to stand at room temperature overnight.
Screening conditions for optimum resolution of MNR26-1 with (-)-dibenzoyl-L-tartaric acid (MNR6-1) to obtain R-di-methoxy-PZQamine (MNR27-x)
* As a result of mnr27-1 not working.
Hazard and Risk Assessment:
As for MNR2-1
MNR27-2
MNR26-1 (0.08 g, 0.3 mmol) and (-)-dibenzoyl-L-tartaric acid. 2IPA (0.15 g, 0.3 mmol) was dissolved in isopropanol (4 mL) in a vial and heated with the heat gun to dissolve the reagents.
Everything went into solution and the vial was left to stand at room temperature overnight.
MNR27-3
MNR26-1 (0.08 g, 0.3 mmol) and (-)-dibenzoyl-L-tartaric acid. 2IPA (0.15 g, 0.3 mmol) was dissolved in hexane (4 mL) in a vial and heated with the heat gun to dissolve the reagents.
very little went into solution and the vial was left to stand at room temperature overnight.
MNR27-4
MNR26-1 (0.08 g, 0.3 mmol) and (-)-dibenzoyl-L-tartaric acid. 2IPA (0.15 g, 0.3 mmol) was dissolved in IPA (1 mL) ans hexane(3 mL) in a vial and heated with the heat gun to dissolve the reagents.
very little went into solution and the vial was left to stand at room temperature overnight.
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