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62026206Attempts to isolate [Yb(OTf)2(R-iPr-pybox)2]+
Experiments
plus.google.com-113014781212630252105Murray Robertson Yb(OTf)3 (0.050 g, 0.08 mmol) and R-iPr-box (0.049 g, 0.16 mmol) in THF (5 mL) in THF (5 mL) was stirred at room temperature for 10 minutes. The solution was then concentrated to about 0.5 mL volume and Et2O (5 mL) was added. A white precipitate appeared but had a very sticky consistency and was not crystalline. The mixture was concentrated to complete dryness]]>


Yb(OTf)3 (0.050 g, 0.08 mmol) and R-iPr-box (0.049 g, 0.16 mmol) in THF (5 mL) in THF (5 mL) was stirred at room temperature for 10 minutes. The solution was then concentrated to about 0.5 mL volume and Et2O (5 mL) was added. A white precipitate appeared but had a very sticky consistency and was not crystalline. The mixture was concentrated to complete dryness
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62027109Attempts to isolate [Yb(OTf)2(R-iPr-pybox)2]+
Experiments
plus.google.com-113014781212630252105Murray Robertson Yb(OTf)3 (0.050 g, 0.08 mmol) and R-iPr-box (0.049 g, 0.16 mmol) in THF (5 mL) in THF (5 mL) was stirred at room temperature for 10 minutes. The solution was then concentrated to about 0.5 mL volume and Et2O (5 mL) was added. A white precipitate appeared but had a very sticky consistency and was not crystalline. The mixture was concentrated to complete dryness]]>


Yb(OTf)3 (0.050 g, 0.08 mmol) and R-iPr-box (0.049 g, 0.16 mmol) in THF (5 mL) in THF (5 mL) was stirred at room temperature for 10 minutes. The solution was then concentrated to about 0.5 mL volume and Et2O (5 mL) was added. A white precipitate appeared but had a very sticky consistency and was not crystalline. The mixture was concentrated to complete dryness
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