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4177Monitoring Template - TLC
Primer
graham-tizzard.myopenid.comGraham TizzardExperiment: Reaction_of_X_and_Y
Lab Book-Expt. Code: 1111-001
Date Of Experiment: 29.06.09
Procedural Step: Monitoring_-_TLC
Post Type: Monitoring
Monitoring Type: TLC
A TLC was run
Plate type: Silica
Eluent type: 95:5 DCM:MeOH.

*** Image Place Holder ***

What Spotted (L-R):-starting material, mixed spot, reaction


Spot (no. from bottom) Height (mm) Rf Visible Short Wave UV Long Wave UV Dip Type Dip Result Inference
Solvent Front281N/AN/AN/AN/AN/AN/A
3260.93yesN/AorangeN/AN/Astarting material
2100.36yes - v. feintN/AblueN/AN/Adecomposition? contaminant?
160.21yesN/AorangeN/AN/Aproduct



Conclusions: no starting material left, reaction gone to completion

Previous Post Reaction of X and Y - Method 1
Linked Posts
This post is linked by:
]]>2009-07-01T10:12:20+01:002009-07-01T15:55:48+01:001b31baedf007caa32a1d07438914587adReaction_of_X_and_Y1111-00129.06.09Monitoring_-_TLCMonitoringTLChttp://www.ourexperiment.org/uri/1chttps://www.ourexperiment.org/labbook_engage/41/Monitoring_Template__TLC.htmlhttps://www.ourexperiment.org/labbook_engage/41/Monitoring_Template__TLC.htmlhttps://www.ourexperiment.org/labbook_engage/41/Monitoring_Template__TLC.xmlhttps://www.ourexperiment.org/labbook_engage/41/Monitoring_Template__TLC.pnghttps://www.ourexperiment.org/labbook_engage/41/Monitoring_Template__TLC.xml?revision=41https://www.ourexperiment.org/labbook_engage/41/Monitoring_Template__TLC.xml?revision=42https://www.ourexperiment.org/labbook_engage/41/Monitoring_Template__TLC.xml?revision=43https://www.ourexperiment.org/labbook_engage/41/Monitoring_Template__TLC.xml?revision=44https://www.ourexperiment.org/labbook_engage/41/Monitoring_Template__TLC.xml?revision=45https://www.ourexperiment.org/labbook_engage/41/Monitoring_Template__TLC.xml?revision=77https://www.ourexperiment.org/labbook_engage/41/Monitoring_Template__TLC.xml?revision=7085
417085Monitoring Template - TLC
Primer
graham-tizzard.myopenid.comGraham TizzardExperiment: Reaction_of_X_and_Y
Lab Book-Expt. Code: 1111-001
Date Of Experiment: 29.06.09
Procedural Step: Monitoring_-_TLC
Post Type: Monitoring
Monitoring Type: TLC
A TLC was run
Plate type: Silica
Eluent type: 95:5 DCM:MeOH.

*** Image Place Holder ***

What Spotted (L-R):-starting material, mixed spot, reaction


Spot (no. from bottom) Height (mm) Rf Visible Short Wave UV Long Wave UV Dip Type Dip Result Inference
Solvent Front281N/AN/AN/AN/AN/AN/A
3260.93yesN/AorangeN/AN/Astarting material
2100.36yes - v. feintN/AblueN/AN/Adecomposition? contaminant?
160.21yesN/AorangeN/AN/Aproduct



Conclusions: no starting material left, reaction gone to completion

Previous Post Reaction of X and Y - Method 1
Linked Entries
This entry is linked by:
]]>2009-07-01T10:12:20+01:002015-06-01T15:33:34+01:001Reaction_of_X_and_Y1111-00129.06.09Monitoring_-_TLCMonitoringTLChttp://www.ourexperiment.org/uri/1chttps://www.ourexperiment.org/labbook_engage/41/Monitoring_Template__TLC.htmlhttps://www.ourexperiment.org/labbook_engage/41/Monitoring_Template__TLC.htmlhttps://www.ourexperiment.org/labbook_engage/41/Monitoring_Template__TLC.xmlhttps://www.ourexperiment.org/labbook_engage/41/Monitoring_Template__TLC.pnghttps://www.ourexperiment.org/labbook_engage/41/Monitoring_Template__TLC.xml?revision=41https://www.ourexperiment.org/labbook_engage/41/Monitoring_Template__TLC.xml?revision=42https://www.ourexperiment.org/labbook_engage/41/Monitoring_Template__TLC.xml?revision=43https://www.ourexperiment.org/labbook_engage/41/Monitoring_Template__TLC.xml?revision=44https://www.ourexperiment.org/labbook_engage/41/Monitoring_Template__TLC.xml?revision=45https://www.ourexperiment.org/labbook_engage/41/Monitoring_Template__TLC.xml?revision=77https://www.ourexperiment.org/labbook_engage/41/Monitoring_Template__TLC.xml?revision=7085https://www.ourexperiment.org/labbook_engage/41/Monitoring_Template__TLC.xml?revision=-1