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1st July 2009 @ 10:12
A TLC was run Plate type: Silica Eluent type: 95:5 DCM:MeOH. [color=red] *** Image Place Holder *** [/color] What Spotted (L-R):-starting material, mixed spot, reaction [table] [mrow] Spot (no. from bottom) [col] Height (mm) [col] Rf [col] Visible [col] Short Wave UV [col] Long Wave UV [col] Dip Type [col] Dip Result [col] Inference [/mrow] [row]Solvent Front[col]28[col]1[col]N/A[col]N/A[col]N/A[col]N/A[col]N/A[col]N/A[/row] [row]3[col]26[col]0.93[col]yes[col]N/A[col]orange[col]N/A[col]N/A[col]starting material[/row] [row]2[col]10[col]0.36[col]yes - v. feint[col]N/A[col]blue[col]N/A[col]N/A[col]decomposition? contaminant?[/row] [row]1[col]6[col]0.21[col]yes[col]N/A[col]orange[col]N/A[col]N/A[col]product[/row] [/table] Conclusions: no starting material left, reaction gone to completion Previous Post [blog]40[/blog]