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30th March 2012 @ 04:13
Attempting to trap the enediamide for analysis and for catalyst screening.

MNR33-1%20scheme.png
mnr33-1%20table.PNG

Hazard and Risk Assessment
HIRAC MNR33.pdf


Procedure
MNR10-2 (0.43 g, 0.94 mmol) in toluene (50 mL) at -78 °C was treated with copper triflate (0.010 g, 0.09 mmol) and stirred at -78 °C. Following the reaction by TLC it looked like PS product was slowly beginning to form after 2 hours and no significant sign of enediamide (expected to a higher running spot on the TLC compared to starting material and PS product)
Attached Files
mnr33-1 table.PNG
MNR33-1 scheme.png
HIRAC MNR33.pdf